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Advanced Characterization and Fine Analysis / Scanning probe microscopy

Atomic Force Microscopy

AFM is a surface sensitive technique permitting to obtain a microscopic image of the topography of a material surface. Typical lateral image sizes are within a range of only a few Nanometers to several 10 Micrometers, whereas height changes of less than a Nanometer may be resolved.

A fine tip attached to a cantilever is scanned across the material surface and enables to measure height changes exploiting an optical beam deflection system (a laser that is reflected from the rear side of the cantilever onto a segmented photodiode). The position of a laser spot on the photodiode permits to track height changes as e.g. due to a nano-particle on the surface or an atomic terrace of a single crystal surface. A feedback loop controls the tip-surface distance and therefore ensures stable imaging conditions.

Different operation modes like contact or non-contact mode can be used to optimize the imaging conditions with highest lateral resolution on one hand and least sample interaction on the other hand. Measurements in different environmental conditions (liquid, gas,...) on a broad class of samples (smooth, rough, insulating, conductive, soft, stiff, wet, dry...) can be performed.

Choosing suitable tips and imaging modes, additional surface properties can be mapped together with the topography, with similar spatial resolution, like friction force, magnetization and surface potential, surface charge density and electrical resistance, as well as elastic modulus and adhesion of heterogeneous sample surfaces can be obtained. 

Available instruments

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Lab's Facility

Milano

POLIFAB

Milano

UNIMI-Fisica

Instruments' description and comparison